(R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid

Base Information

• Chemical Name: (R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid
• CAS No.: 154003-64-2
• Molecular Formula: C₁₃H₁₆ClN₃O₄
• Molecular Weight: 313.741

Synonyms:(R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid

Chemical Property of (R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid

Chemical Property:

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Technology Process of (R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid

There total 3 articles about (R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid (154334-37-9) → (R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid (154003-64-2)

Guidance literature:

With sodium hydroxide; dihydrogen peroxide; In methanol;

DOI:10.1002/ardp.19933260911

Reference yield:

4-chloro-N-methyl-2-nitroaniline (15950-17-1) → (R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid (154003-64-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / pyridine / Heating

2: 89 percent / 30percent H₂O₂, 0.5N NaOH / methanol

With sodium hydroxide; dihydrogen peroxide; In pyridine; methanol;

DOI:10.1002/ardp.19933260911

Reference yield:

(R)-(+)-Ethylmethylcyanessigsaeurechlorid → (R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-malonsaeurediamid (154003-64-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 94 percent / pyridine / Heating

2: 89 percent / 30percent H₂O₂, 0.5N NaOH / methanol

With sodium hydroxide; dihydrogen peroxide; In pyridine; methanol;

DOI:10.1002/ardp.19933260911

upstream raw materials:

(R)-(-)-N-<4-Chlor-2-nitro-phenyl>-N-methyl-ethyl-methyl-cyanessigsaeureamid

4-chloro-N-methyl-2-nitroaniline

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