C₆H₅N{P(OC₆H₃(OMe-o)(C₃H₅-p))2}2

Base Information

• Chemical Name: C₆H₅N{P(OC₆H₃(OMe-o)(C₃H₅-p))2}2
• CAS No.: 1256288-89-7
• Molecular Formula: C₄₆H₄₉NO₈P₂
• Molecular Weight: 805.844
• Mol file: 1256288-89-7.mol

Synonyms:C₆H₅N{P(OC₆H₃(OMe-o)(C₃H₅-p))2}2

Chemical Property of C₆H₅N{P(OC₆H₃(OMe-o)(C₃H₅-p))2}2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆H₅N{P(OC₆H₃(OMe-o)(C₃H₅-p))2}2

There total 1 articles about C₆H₅N{P(OC₆H₃(OMe-o)(C₃H₅-p))2}2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

4-allylguaiacol (97-53-0) + N,N'-bis(dichlorophosphino)aniline (39652-40-9) → C6H5N{P(OC6H3(OMe-o)(C3H5-p))2}2 (1256288-89-7)

Guidance literature:

With triethylamine; In diethyl ether; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.ica.2010.03.030

Reference yield: 94.0%

bis(dicarbonyl(η-cyclopentadienyl)iron) + C6H5N{P(OC6H3(OMe-o)(C3H5-p))2}2 (1256288-89-7) → [CpFe(CO)(PhNH(P(OC6H3(OMe-o)(C3H5-p))2))(P(O)(OC6H3(OMe-o)(C3H5-p))]

Guidance literature:

In toluene; under N2 or Ar; mixt. of Fe compd. and aminobis(phosphonite) (1:1 molar ratio) in toluene refluxed for 2 h; soln. filtered, filtrate evapd., residue washed with petroleum ether, dried under vac.; elem. anal.;

DOI:10.1016/j.ica.2010.03.030

Reference yield: 87.0%

C6H5N{P(OC6H3(OMe-o)(C3H5-p))2}2 (1256288-89-7) + copper(l) chloride → [Cu2(μ-Cl)(μ3-Cl){C6H5N{P(OC6H3(OMe-o)(C3H5-p))2}2}]2 (1580528-45-5)

Guidance literature:

In acetonitrile; for 4h; Schlenk technique; Inert atmosphere;

DOI:10.1021/ic500240j

upstream raw materials:

4-allylguaiacol

N,N'-bis(dichlorophosphino)aniline

Downstream raw materials:

[Au₂Cl₂(PhN(P(OC₆H₃(OMe-o)(C₃H₅-p))2)2)]

cis-[Mo(CO)4(N,N-bis(bis(2-methoxy-4-allyl-phenyloxy)phosphino)aniline)

cis-[W(CO)4(N,N-bis(bis(2-methoxy-4-allyl-phenyloxy)phosphino)aniline)

[(η6-p-cymene)(μ-Cl)3Ru2Cl(PhN(P(OC6H3(OMe-o)(C3H5-p))2)2)]