N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol

Base Information

• Chemical Name: N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol
• CAS No.: 1610419-76-5
• Molecular Formula: C₂₂H₃₃N₅O
• Molecular Weight: 383.537

Synonyms:N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol

Chemical Property of N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol

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Technology Process of N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol

There total 1 articles about N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

1-Methylhomopiperazine (4318-37-0) + N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)[(3-chloro)(2-hydroxy)] propylamine (1610419-77-6) → N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol (1610419-76-5)

Guidance literature:

1-Methylhomopiperazine; N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)[(3-chloro)(2-hydroxy)] propylamine; In acetonitrile; at 20 ℃; for 48h;

In acetonitrile; at 40 ℃; for 72h;

DOI:10.1007/s11243-013-9791-8

Reference yield: 72.0%

zinc perchlorate + ethanol (64-17-5) + 3,5-dinitrobenzoic acid (99-34-3) + N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol (1610419-76-5) + sodium tetraphenyl borate (143-66-8) → C36H38N9O13Zn2(1+)*C24H20B(1-)*C2H6O

Guidance literature:

zinc perchlorate; N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol; With triethylamine; In methanol; at 20 ℃; for 1h;

3,5-dinitrobenzoic acid; With triethylamine; In methanol; at 20 ℃; for 1h;

ethanol; sodium tetraphenyl borate; Further stages;

DOI:10.1002/zaac.201500196

Reference yield: 70.0%

nickel(II) perchlorate hexahydrate + N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol (1610419-76-5) + water (7732-18-5) + sodium diphenyl phosphate (3279-55-8) → [Ni2(N-4-methylhomopiperazine-N'-[N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)amine]-1,3-diaminopropan-2-ol(-H))(bisphenyl phosphate)2][ClO4]*2H2O

Guidance literature:

With triethylamine; In methanol; at 20 ℃; for 1h;

DOI:10.1007/s11243-013-9791-8

upstream raw materials:

1-Methylhomopiperazine

N-(2-pyridylmethyl)-N-2-(2-pyridylethyl)[(3-chloro)(2-hydroxy)] propylamine

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