[(S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane

Base Information

Chemical Name:[(S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane
CAS No.:130626-36-7
Molecular Formula:C₂₃H₄₂O₆Si
Molecular Weight:442.668
Hs Code.:

Synonyms:[(S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane

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Chemical Property of [(S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane

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Technology Process of [(S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane

There total 11 articles about [(S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 130626-35-6
(3S)-5-<(benzyloxy)methoxy>-3-<(2-methoxyethoxy)methoxy>-2-pentanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 130626-36-7
[(S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 90 ℃; for 12h; Title compound not separated from byproducts;
DOI:10.1016/S0040-4020(01)81517-9

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 130626-36-7
[(1R,2S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: iPr₂NEt / Ambient temperature

2: Zn(BH₄)2 / diethyl ether / -78 °C

3: 1.) Zn(BH₄)2; 2.) ImH / 1.) -78 degC, ether; 2.) 90 degC, DMF

With 1H-imidazole; zinc(II) tetrahydroborate; N-ethyl-N,N-diisopropylamine; In diethyl ether;
DOI:10.1246/cl.1987.2097

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 130626-36-7
[(1S,2S)-4-Benzyloxymethoxy-2-(2-methoxy-ethoxymethoxy)-1-methyl-butoxy]-tert-butyl-dimethyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: iPr₂NEt / Ambient temperature

2: Zn(BH₄)2 / diethyl ether / -78 °C

3: 1.) Zn(BH₄)2; 2.) ImH / 1.) -78 degC, ether; 2.) 90 degC, DMF

With 1H-imidazole; zinc(II) tetrahydroborate; N-ethyl-N,N-diisopropylamine; In diethyl ether;
DOI:10.1246/cl.1987.2097