1-(3-dodecyloxyphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium bromide

Base Information

• Chemical Name: 1-(3-dodecyloxyphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium bromide
• CAS No.: 1179810-96-8
• Molecular Formula: Br*C₂₉H₄₁N₂O₅
• Molecular Weight: 577.559
• Mol file: 1179810-96-8.mol

Synonyms:1-(3-dodecyloxyphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium bromide

Chemical Property of 1-(3-dodecyloxyphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 1-(3-dodecyloxyphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium bromide

There total 1 articles about 1-(3-dodecyloxyphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

1-(3-dodecyloxyphenyl)-1-hydroxy-1,2-dihydropyrrolo[3,4-c]pyridine-3-one (1179810-88-8) + ethyl bromoacetate (105-36-2) → 1-(3-dodecyloxyphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium bromide (1179810-96-8)

Guidance literature:

In tetrahydrofuran; Reflux; Inert atmosphere;

DOI:10.1016/j.ejmech.2010.07.016

Reference yield: 51.0%

1-(3-dodecyloxyphenyl)-5-[2-(ethyloxy)-2-oxoethyl]-1-hydroxy-3-oxo-1,2-dihydropyrrolo[3,4-c]pyridinium bromide (1179810-96-8) → ethyl 3-aminocarbonyl-[4-(3-dodecyloxybenzoyl)-1,4-dihydropyridin-1-yl]acetate

Guidance literature:

With sodium tris(acetoxy)borohydride; In ethanol; acetic acid; at 0 ℃; for 0.166667h; Inert atmosphere;

DOI:10.1016/j.ejmech.2010.07.016

upstream raw materials:

1-(3-dodecyloxyphenyl)-1-hydroxy-1,2-dihydropyrrolo[3,4-c]pyridine-3-one

ethyl bromoacetate