(S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one

Base Information

Chemical Name:(S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one
CAS No.:1307885-09-1
Molecular Formula:C₂₄H₂₃N₃OS
Molecular Weight:401.532
Hs Code.:

Synonyms:(S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one

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Chemical Property of (S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one

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Technology Process of (S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one

There total 3 articles about (S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1307885-07-9
(6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate

: 1307885-09-1
(S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one

Guidance literature:: With hydrogenchloride; In methanol; acetic acid; at 100 ℃; for 3h;
DOI:10.1039/c0ob01083a

Reference yield:

: 37088-66-7
(3S)-methyl 3-amino-3-phenylpropanoate

: 1307885-09-1
(S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / dichloromethane; water / 0.17 h / 0 °C

1.2: 1 h / 20 °C

2.1: dichloromethane / 20 °C

3.1: hydrogenchloride / methanol; acetic acid / 3 h / 100 °C

With hydrogenchloride; sodium hydrogencarbonate; In methanol; dichloromethane; water; acetic acid;
DOI:10.1039/c0ob01083a

Reference yield:

: C₁₁H₁₁NO₂S

: tert-Butyl [(1S,2S)-2-amino-1,2-diphenylethyl]carbamate

: 1307885-09-1
(S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 20 °C

2: hydrogenchloride / methanol; acetic acid / 3 h / 100 °C

With hydrogenchloride; In methanol; dichloromethane; acetic acid;
DOI:10.1039/c0ob01083a