(6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate

Base Information

• Chemical Name: (6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate
• CAS No.: 1307885-07-9
• Molecular Formula: C₃₀H₃₅N₃O₄S
• Molecular Weight: 533.692

Synonyms:(6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate

Chemical Property of (6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate

Chemical Property:

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Technology Process of (6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate

There total 2 articles about (6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(3S)-methyl 3-amino-3-phenylpropanoate (37088-66-7) → (6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate (1307885-07-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / dichloromethane; water / 0.17 h / 0 °C

1.2: 1 h / 20 °C

2.1: dichloromethane / 20 °C

With sodium hydrogencarbonate; In dichloromethane; water;

DOI:10.1039/c0ob01083a

Reference yield:

C11H11NO2S + tert-Butyl [(1S,2S)-2-amino-1,2-diphenylethyl]carbamate → (6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate (1307885-07-9)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1039/c0ob01083a

Reference yield: 93.0%

(6S,7S,11S)-methyl 2,2-dimethyl-4-oxo-6,7,11-triphenyl-9-thioxo-3-oxa-5,8,10-triazatridecan-13-oate (1307885-07-9) → (S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one (1307885-09-1)

Guidance literature:

With hydrogenchloride; In methanol; acetic acid; at 100 ℃; for 3h;

DOI:10.1039/c0ob01083a

upstream raw materials:

(3S)-methyl 3-amino-3-phenylpropanoate

Downstream raw materials:

(S)-3-[(1S,2S)-2-amino-1,2-diphenylethyl]-6-phenyl-2-thiotetrahydropyrimidin-4-(1H)-one

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