C₅₈H₇₀N₈O₁₃Si

Base Information

Chemical Name:C₅₈H₇₀N₈O₁₃Si
CAS No.:334832-30-3
Molecular Formula:C₅₈H₇₀N₈O₁₃Si
Molecular Weight:1115.33
Hs Code.:

C<sub>58</sub>H<sub>70</sub>N<sub>8</sub>O<sub>13</sub>Si

Synonyms:C₅₈H₇₀N₈O₁₃Si

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Chemical Property of C₅₈H₇₀N₈O₁₃Si

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Technology Process of C₅₈H₇₀N₈O₁₃Si

There total 20 articles about C₅₈H₇₀N₈O₁₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₉H₇₄N₈O₁₆SSi

: 334832-30-3
C₅₈H₇₀N₈O₁₃Si

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In chloroform; at 0 ℃; for 0.5h;
DOI:10.1246/cl.2001.102

Reference yield:

: 334832-21-2
(S)-5,2',2'-Trimethyl-4',5'-dihydro-[2,4']bioxazolyl-4,3'-dicarboxylic acid 3'-benzyl ester 4-methyl ester

: 334832-30-3
C₅₈H₇₀N₈O₁₃Si

Guidance literature:: Multi-step reaction with 11 steps

1: LiOH / methanol

2: diphenylphosphoryl azide; Et₃N / dimethylformamide / 7 h / 0 - 20 °C

3: 85 percent / TFA / CHCl₃ / 1.5 h / 0 - 20 °C

4: 89 percent / imidazole / CH₂Cl₂ / 2 h / 0 - 20 °C

5: H₂ / Pd-C / ethanol / 1 h / 20 °C

6: 67 percent / BOP; (i-Pr)2NEt / CH₂Cl₂ / 13 h / 0 - 20 °C

7: Et₃N / CHCl₃ / 0.5 h / 0 °C

8: DBU / CHCl₃ / 0.5 h / 0 °C

9: 89 percent / AcOH / tetrahydrofuran; H₂O / 0.5 h / 20 °C

10: Et₃N / CHCl₃ / 0.5 h / 0 °C

11: DBU / CHCl₃ / 0.5 h / 0 °C

With 1H-imidazole; lithium hydroxide; diphenylphosphoranyl azide; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1246/cl.2001.102

Reference yield:

: 334832-22-3
(S)-5,2',2'-Trimethyl-4',5'-dihydro-[2,4']bioxazolyl-4,3'-dicarboxylic acid 3'-benzyl ester

: 334832-30-3
C₅₈H₇₀N₈O₁₃Si

Guidance literature:: Multi-step reaction with 10 steps

1: diphenylphosphoryl azide; Et₃N / dimethylformamide / 7 h / 0 - 20 °C

2: 85 percent / TFA / CHCl₃ / 1.5 h / 0 - 20 °C

3: 89 percent / imidazole / CH₂Cl₂ / 2 h / 0 - 20 °C

4: H₂ / Pd-C / ethanol / 1 h / 20 °C

5: 67 percent / BOP; (i-Pr)2NEt / CH₂Cl₂ / 13 h / 0 - 20 °C

6: Et₃N / CHCl₃ / 0.5 h / 0 °C

7: DBU / CHCl₃ / 0.5 h / 0 °C

8: 89 percent / AcOH / tetrahydrofuran; H₂O / 0.5 h / 20 °C

9: Et₃N / CHCl₃ / 0.5 h / 0 °C

10: DBU / CHCl₃ / 0.5 h / 0 °C

With 1H-imidazole; diphenylphosphoranyl azide; hydrogen; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1246/cl.2001.102