C₁₅H₁₁BrClNO

Base Information

• Chemical Name: C₁₅H₁₁BrClNO
• CAS No.: 1373937-42-8
• Molecular Formula: C₁₅H₁₁BrClNO
• Molecular Weight: 336.615
• Mol file: 1373937-42-8.mol

Synonyms:C₁₅H₁₁BrClNO

Chemical Property of C₁₅H₁₁BrClNO

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₅H₁₁BrClNO

There total 3 articles about C₁₅H₁₁BrClNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-1-(4-bromophenyl)-3-(4-chlorophenyl)-prop-2-en-1-one (126443-16-1) → C15H11BrClNO (1373937-42-8)

Guidance literature:

With pyridine; hydroxylamine hydrochloride; In methanol; at 25 ℃; Inert atmosphere;

DOI:10.1002/anie.201301963

Reference yield:

para-bromoacetophenone (99-90-1) → C15H11BrClNO (1373937-42-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / methanol; water / 25 °C / Inert atmosphere

2: hydroxylamine hydrochloride; pyridine / methanol / 25 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; potassium hydroxide; In methanol; water;

DOI:10.1002/anie.201301963

Reference yield:

4-chlorobenzaldehyde (104-88-1) → C15H11BrClNO (1373937-42-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxide / methanol; water / 25 °C / Inert atmosphere

2: hydroxylamine hydrochloride; pyridine / methanol / 25 °C / Inert atmosphere

With pyridine; hydroxylamine hydrochloride; potassium hydroxide; In methanol; water;

DOI:10.1002/anie.201301963

upstream raw materials:

(E)-1-(4-bromophenyl)-3-(4-chlorophenyl)-prop-2-en-1-one

para-bromoacetophenone

4-chlorobenzaldehyde

Refernces