C₁₃H₁₉NO₃S

Base Information

Chemical Name:C₁₃H₁₉NO₃S
CAS No.:1352347-71-7
Molecular Formula:C₁₃H₁₉NO₃S
Molecular Weight:269.365
Hs Code.:

C<sub>13</sub>H<sub>19</sub>NO<sub>3</sub>S

Synonyms:C₁₃H₁₉NO₃S

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Chemical Property of C₁₃H₁₉NO₃S

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Technology Process of C₁₃H₁₉NO₃S

There total 11 articles about C₁₃H₁₉NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 202743-07-5
(2S,3R)-1-benzyl-2-methylpyrrolidin-3-ol

: 124-63-0
methanesulfonyl chloride

: 1352347-71-7
C₁₃H₁₉NO₃S

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.tet.2011.07.049

Reference yield: 81.0%

: C₁₂H₁₉NO₂

: 124-63-0
methanesulfonyl chloride

: 1352347-71-7
C₁₃H₁₉NO₃S

Guidance literature:: With dmap; C₁₂H₁₉NO₂; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1248/cpb.c16-00568

Reference yield:

: 1294446-91-5
(S)-tert-butyl-N-(3-oxohex-5-en-2-yl)carbamate

: 1352347-71-7
C₁₃H₁₉NO₃S

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium tetrahydroborate / ethanol / 20 °C

2.1: 1H-imidazole; dmap / N,N-dimethyl-formamide / 0 - 20 °C

3.1: sodium periodate; ruthenium(III) trichloride hydrate / tetrachloromethane; water; acetonitrile / 16 h / 20 °C

4.1: trifluoroacetic acid / dichloromethane / 4 h / 0 - 20 °C

4.2: 0 °C

5.1: sodium hydride / N,N-dimethyl-formamide / 0 °C

5.2: 2.5 h / 0 - 20 °C

6.1: methanol; thionyl chloride / 2 h / 0 - 20 °C

7.1: dimethylsulfide borane complex / tetrahydrofuran / 20 h / 0 - 20 °C

8.1: dmap; triethylamine / dichloromethane / 3 h / 0 - 20 °C

With 1H-imidazole; methanol; dmap; sodium tetrahydroborate; sodium periodate; thionyl chloride; ruthenium(III) trichloride hydrate; dimethylsulfide borane complex; sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2011.07.049