4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 3,3-difluoro-2-(4-methoxyphenyl)amino-2-(2-methylallyl)-5-hexenoate

Base Information

Chemical Name:4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 3,3-difluoro-2-(4-methoxyphenyl)amino-2-(2-methylallyl)-5-hexenoate
CAS No.:1071528-21-6
Molecular Formula:C₂₈H₂₆F₁₉NO₃
Molecular Weight:785.489
Hs Code.:

Synonyms:4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 3,3-difluoro-2-(4-methoxyphenyl)amino-2-(2-methylallyl)-5-hexenoate

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Chemical Property of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 3,3-difluoro-2-(4-methoxyphenyl)amino-2-(2-methylallyl)-5-hexenoate

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Technology Process of 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 3,3-difluoro-2-(4-methoxyphenyl)amino-2-(2-methylallyl)-5-hexenoate

There total 1 articles about 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 3,3-difluoro-2-(4-methoxyphenyl)amino-2-(2-methylallyl)-5-hexenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1458-98-6
2-methyl-3-bromo-1-propene

: 1039136-82-7
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (E)-3,3-difluoro-2-[(4-methoxyphenyl)imino]-5-hexenoate

: 1071528-21-6
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 3,3-difluoro-2-(4-methoxyphenyl)amino-2-(2-methylallyl)-5-hexenoate

Guidance literature:: 2-methyl-3-bromo-1-propene; With zinc; In tetrahydrofuran; at 50 ℃; for 0.75h; Inert atmosphere;

4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl (E)-3,3-difluoro-2-[(4-methoxyphenyl)imino]-5-hexenoate; In tetrahydrofuran; at -40 ℃; chemoselective reaction; Inert atmosphere;
DOI:10.1002/chem.200702009

Reference yield: 80.0%

: 1071528-21-6
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 3,3-difluoro-2-(4-methoxyphenyl)amino-2-(2-methylallyl)-5-hexenoate

: 1071528-30-7
4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoroundecyl 6,6-difluoro-1-((4-methoxyphenyl)amino)-3-methyl-3-cyclohexene-1-carboxylate

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; Inert atmosphere; Reflux;
DOI:10.1002/chem.200702009