Technology Process of C18H19F2N5O*ClH
There total 7 articles about C18H19F2N5O*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride; hydrogen;
5%-palladium/activated carbon;
In
ethanol; water;
for 1h;
under 775.743 Torr;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: pyridine / dmap / toluene / 24 h / 20 °C / Inert atmosphere
2: sodium hydride; methanol / toluene; mineral oil / 7 h / 65 °C
3: hydrogenchloride; hydrogen / 5%-palladium/activated carbon / ethanol; water / 1 h / 775.74 Torr
With
pyridine; hydrogenchloride; methanol; hydrogen; sodium hydride;
dmap; 5%-palladium/activated carbon;
In
ethanol; water; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: hydrogen / acetic acid; platinum(IV) oxide / isopropyl alcohol / 12 h / 20 °C / 2585.81 Torr
2: dichloromethane / 12 h / 20 °C
3: triethylamine / ethanol / 2 h / 50 °C
4: ammonia; dihydrogen peroxide / ethanol; water / 2.17 h / 20 °C
5: pyridine / dmap / toluene / 24 h / 20 °C / Inert atmosphere
6: sodium hydride; methanol / toluene; mineral oil / 7 h / 65 °C
7: hydrogenchloride; hydrogen / 5%-palladium/activated carbon / ethanol; water / 1 h / 775.74 Torr
With
pyridine; hydrogenchloride; methanol; ammonia; hydrogen; dihydrogen peroxide; sodium hydride; triethylamine;
dmap; platinum(IV) oxide; 5%-palladium/activated carbon; acetic acid;
In
ethanol; dichloromethane; water; isopropyl alcohol; toluene; mineral oil;
