(1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol

Base Information

Chemical Name:(1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol
CAS No.:204004-80-8
Molecular Formula:C₁₆H₃₁N₃O₂Si
Molecular Weight:325.527
Hs Code.:

Synonyms:(1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol

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Chemical Property of (1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol

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Technology Process of (1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol

There total 4 articles about (1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 67373-56-2
chlorodimethyl(1,1,2-trimethylpropyl)silane

: 204004-79-5
(1S,2R)-3-(2-Azidoethyl)cyclohex-3-ene-1,2-diol

: 204004-80-8
(1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 13h;
DOI:10.1055/s-1998-4529

Reference yield:

: 6926-44-9
phenethyl azide

: 204004-80-8
(1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol

Guidance literature:: Multi-step reaction with 3 steps

1: Escherichia coli JM₁₀₉(pDTG₆₀₁)

2: 72 percent / potassium azodicarboxylate, HOAc / methanol / 14 h / Ambient temperature

3: 99 percent / imidazole / dimethylformamide / 13 h / 0 °C

With 1H-imidazole; Escherichia coli JM₁₀₉(pDTG₆₀₁); potassium diazodicarboxylate; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-1998-4529

Reference yield:

: 103-63-9
1-phenyl-2-bromoethane

: 204004-80-8
(1R,6S)-2-(2-Azido-ethyl)-6-[dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-cyclohex-2-enol

Guidance literature:: Multi-step reaction with 4 steps

1: NaN₃ / dimethylformamide

2: Escherichia coli JM₁₀₉(pDTG₆₀₁)

3: 72 percent / potassium azodicarboxylate, HOAc / methanol / 14 h / Ambient temperature

4: 99 percent / imidazole / dimethylformamide / 13 h / 0 °C

With 1H-imidazole; sodium azide; Escherichia coli JM₁₀₉(pDTG₆₀₁); potassium diazodicarboxylate; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1055/s-1998-4529