3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole

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Chemical Name:3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole
CAS No.:1219617-49-8
Molecular Formula:C₂₃H₃₉NO₃Si
Molecular Weight:405.653
Hs Code.:

Synonyms:3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole

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Chemical Property of 3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole

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Technology Process of 3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole

There total 1 articles about 3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1219617-48-7
C₂₁H₃₅NO₃Si

: 74-88-4
methyl iodide

: 1219617-49-8
3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole

Guidance literature:: C₂₁H₃₅NO₃Si; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; mineral oil; at 0 - 25 ℃; Inert atmosphere;
DOI:10.1021/ol100333d

Reference yield: 65.0%

: 1219617-49-8
3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole

: 1219617-50-1
3-methoxy-α-methyl-5-phenyl-1H-pyrrole-2-butanol

Guidance literature:: With hydrogen fluoride; In tetrahydrofuran; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo402178r

Reference yield: 41.0%

: 1219617-49-8
3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole

: 1219617-50-1
3-methoxy-α-methyl-5-phenyl-1H-pyrrole-2-butanol

: (±)-(4R,5S,7R)-4-methoxy-7-methyl-2-phenyl-6-oxa-1-azaspiro[4.5]dec-1-ene

: (±)-(4S,5R,7R)-4-methoxy-7-methyl-2-phenyl-6-oxa-1-azaspiro[4.5]dec-1-ene

: (±)-(4R,5R,7R)-4-methoxy-7-methyl-2-phenyl-6-oxa-1-azaspiro[4.5]dec-1-ene

Guidance literature:: 3,4-dihydro-2,3-dimethoxy-2-(4-triethylsilyloxypentyl)-5-phenyl-2H-pyrrole; With hydrogenchloride; water; In tetrahydrofuran; acetonitrile; at 0 ℃; for 0.666667h; Inert atmosphere;

With sodium hydrogencarbonate; In tetrahydrofuran; water; acetonitrile; pH=7; Inert atmosphere;
DOI:10.1021/ol100333d