phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside
CAS No.:1283073-21-1
Molecular Formula:C₁₈H₂₅N₃O₆S
Molecular Weight:411.479
Hs Code.:

Synonyms:phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 431-03-8
dimethylglyoxal

: 166516-67-2
phenyl 2-azido-2-deoxy-1-thio-β-D-glucopyranoside

: 149-73-5
trimethyl orthoformate

: 1283073-21-1
phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With camphorsulfonic acid; Reflux;
DOI:10.1021/jo102411j

Reference yield: 100.0%

: 1283073-21-1
phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside

: 98-59-9
p-toluenesulfonyl chloride

: 1283073-23-3
phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-6-O-toluenesulfonyl-β-D-glucopyranoside

Guidance literature:: With N,N,N,N,-tetramethylethylenediamine; In acetonitrile; at 20 ℃;
DOI:10.1021/jo102411j

Reference yield: 62.0%

: 1283073-21-1
phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside

: 1283073-30-2
phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside S-oxide

: 1283073-42-6
C₄₈H₅₈N₆O₁₃S

Guidance literature:: phenyl 2-azido-2-deoxy-3,4-O-(2,3-dimethoxybutane-2,3-diyl)-1-thio-β-D-glucopyranoside; phenyl 2-azido-2-deoxy-3,4,6-tri-O-(p-methoxybenzyl)-1-thio-β-D-glucopyranoside S-oxide; With 2,4,6-tri-tertbutylpyridine; In dichloromethane; acetonitrile; at 20 ℃; for 0.5h; Molecular sieve;

With trifluoromethylsulfonic anhydride; In dichloromethane; acetonitrile; at -80 ℃; Molecular sieve;
DOI:10.1021/jo102411j