((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester

Base Information

Chemical Name:((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester
CAS No.:874811-52-6
Molecular Formula:C₂₄H₃₅BrN₂O₄
Molecular Weight:495.457
Hs Code.:

Synonyms:((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester

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Chemical Property of ((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester

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Technology Process of ((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester

There total 1 articles about ((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1611-56-9
1-Bromo-11-hydroxyundecane

: 5262-10-2
[(2S,5S)-5-benzyl-3,6-dioxopiperazin-2-yl]acetic acid

: 874811-52-6
((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester

Guidance literature:: With 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide; In N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1246/bcsj.78.2069

Reference yield: 84.0%

: 110-86-1
pyridine

: 874811-52-6
((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester

: 1-{11-[2-((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetoxy]-undecyl}-pyridinium; bromide

Guidance literature:: at 90 ℃;
DOI:10.1246/bcsj.78.2069

Reference yield: 65.0%

: 874811-52-6
((2S,5S)-5-Benzyl-3,6-dioxo-piperazin-2-yl)-acetic acid 11-bromo-undecyl ester

: 148-24-3,24804-14-6
8-quinolinol

: C₃₃H₄₁N₃O₅

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 40 ℃; Inert atmosphere;
DOI:10.1246/bcsj.20160232