C₃₄H₆₁NO₇Si₂

Base Information

Chemical Name:C₃₄H₆₁NO₇Si₂
CAS No.:1254369-13-5
Molecular Formula:C₃₄H₆₁NO₇Si₂
Molecular Weight:652.032
Hs Code.:

C<sub>34</sub>H<sub>61</sub>NO<sub>7</sub>Si<sub>2</sub>

Synonyms:C₃₄H₆₁NO₇Si₂

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Chemical Property of C₃₄H₆₁NO₇Si₂

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Technology Process of C₃₄H₆₁NO₇Si₂

There total 12 articles about C₃₄H₆₁NO₇Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254369-14-6
C₂₁H₄₆O₄Si₂

: 101711-78-8,131685-53-5
(3R)-3-propionyl-4-benzyloxazolidin-2-one

: 1254369-13-5
C₃₄H₆₁NO₇Si₂

Guidance literature:: With di-n-butylboryl trifluoromethanesulfonate; triethylamine; In dichloromethane; at -78 - 0 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ml1002184

Reference yield:

: 117643-47-7
C₁₃H₁₈O₂

: 1254369-13-5
C₃₄H₆₁NO₇Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: toluene / 36 h / Reflux

2.1: lithium aluminium tetrahydride / diethyl ether / 0.17 h / 0 °C / Inert atmosphere

3.1: 1H-imidazole / N,N-dimethyl-formamide / 16 h / Inert atmosphere

4.1: potassium osmate(VI) dihydrate; methanesulfonamide; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 36 h / 0 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

6.1: N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 0 - 20 °C / Inert atmosphere

7.1: palladium 10% on activated carbon; hydrogen / ethanol

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: -78 - 20 °C

9.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

With 1H-imidazole; potassium osmate(VI) dihydrate; lithium aluminium tetrahydride; oxalyl dichloride; methanesulfonamide; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; potassium carbonate; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; potassium hexacyanoferrate(III); In diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; tert-butyl alcohol; 1.1: Johnson-Claisen orthoester rearrangement / 4.1: Sharpless dihydroxylation / 8.1: Swern oxidation / 8.2: Swern oxidation / 9.1: Evans aldol reaction;
DOI:10.1021/ml1002184

Reference yield:

: 1254369-11-3
(8R,9R)-9-(2-(benzyloxy)ethyl)-11,11-diethyl-8-methoxy-2,2,3,3,8-pentamethyl-4,10-dioxa-3,11-disilatridecane

: 1254369-13-5
C₃₄H₆₁NO₇Si₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

2.2: -78 - 20 °C

3.1: di-n-butylboryl trifluoromethanesulfonate; triethylamine / dichloromethane / -78 - 0 °C / Inert atmosphere

With oxalyl dichloride; di-n-butylboryl trifluoromethanesulfonate; palladium 10% on activated carbon; hydrogen; dimethyl sulfoxide; triethylamine; In ethanol; dichloromethane; 2.1: Swern oxidation / 2.2: Swern oxidation / 3.1: Evans aldol reaction;
DOI:10.1021/ml1002184