tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate

Base Information

Chemical Name:tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate
CAS No.:312719-50-9
Molecular Formula:C₁₇H₂₉N₂O₄P
Molecular Weight:356.402
Hs Code.:

Synonyms:tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate

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Chemical Property of tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate

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Technology Process of tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate

There total 3 articles about tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 142-25-6
N,N',N'-trimethylenediamine

: 312719-37-2
tetrahydrofurfuryl benzyl phosphorochloridate

: 312719-50-9
tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate

Guidance literature:: In acetonitrile; at 20 ℃; for 1h;
DOI:10.1021/jm000302b

Reference yield:

: 97-99-4
Tetrahydrofurfuryl alcohol

: 312719-50-9
tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / POCl₃; Et₃N / CH₂Cl₂ / 0.33 h / -40 - 20 °C

2: 55 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

3: 75 percent / acetonitrile / 1 h / 20 °C

With triethylamine; trichlorophosphate; In dichloromethane; acetonitrile;
DOI:10.1021/jm000302b

Reference yield:

: 312719-40-7
tetrahydrofurfuryl phosphorodichloridate

: 312719-50-9
tetrahydrofurfuryl benzyl N-methyl-N-(2-dimethylaminoethyl)phosphoramidate

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / Et₃N / CH₂Cl₂ / 1 h / 0 °C

2: 75 percent / acetonitrile / 1 h / 20 °C

With triethylamine; In dichloromethane; acetonitrile;
DOI:10.1021/jm000302b