[2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester

Base Information

Chemical Name:[2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester
CAS No.:1083007-61-7
Molecular Formula:C₁₈H₁₇N₅O₃
Molecular Weight:351.365
Hs Code.:

Synonyms:[2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester

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Chemical Property of [2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester

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Technology Process of [2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester

There total 1 articles about [2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 64210-67-9
ethyl 3-oxo-3-(pyrimidin-4-yl)propanoate

: 1083008-47-2
(2-Carbamimidoyl-ethyl)-carbamic acid benzyl ester hydrochloride

: 1083007-61-7
[2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester

Guidance literature:: With sodium hydroxide; In ethanol; for 12h; Heating / reflux;

Reference yield: 64.0%

: 1083007-61-7
[2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester

: 74-88-4
methyl iodide

: 1083007-63-9
[2-(1-methyl-6-oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester

Guidance literature:: [2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;

Reference yield:

: 1083007-61-7
[2-(6-Oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-carbamic acid benzyl ester

: 1083007-50-4
· 4-Chloro-2-methoxy-N-[2-(1-methyl-6-oxo-1,6-dihydro-[4,4']bipyrimidinyl-2-yl)-ethyl]-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.25 h / 20 °C

1.2: 3 h / 0 - 20 °C

2.1: hydrogen bromide; acetic acid / 2 h / 20 °C

3.1: diethyl cyanophosphonate; triethylamine / N,N-dimethyl-formamide / 1 h / 0 - 20 °C

With diethyl cyanophosphonate; hydrogen bromide; potassium carbonate; acetic acid; triethylamine; In N,N-dimethyl-formamide;