benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.0²'⁷.0¹⁴'¹⁸]pentacosa-1⁽²⁵⁾,2,4,6,21,23-hexaen-12-yl]carbamate

Base Information

• Chemical Name: benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.0²'⁷.0¹⁴'¹⁸]pentacosa-1⁽²⁵⁾,2,4,6,21,23-hexaen-12-yl]carbamate
• CAS No.: 1460301-50-1
• Molecular Formula: C₃₇H₃₆N₄O₇
• Molecular Weight: 648.715

Synonyms:benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.0²'⁷.0¹⁴'¹⁸]pentacosa-1⁽²⁵⁾,2,4,6,21,23-hexaen-12-yl]carbamate

Chemical Property of benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.0²'⁷.0¹⁴'¹⁸]pentacosa-1⁽²⁵⁾,2,4,6,21,23-hexaen-12-yl]carbamate

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Technology Process of benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.0²'⁷.0¹⁴'¹⁸]pentacosa-1⁽²⁵⁾,2,4,6,21,23-hexaen-12-yl]carbamate

There total 14 articles about benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.0²'⁷.0¹⁴'¹⁸]pentacosa-1⁽²⁵⁾,2,4,6,21,23-hexaen-12-yl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

benzyl N-[(12R,16S,18S)-16-amino-8,13-dioxo-20-oxa-9,14-diazatetracyclo[19.3.1.02'7.014'18]pentacosa-1(25),2,4,6,21,23-hexaen-12-yl]carbamate hydrochloride + phenyl chloroformate (1885-14-9) → benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.02'7.014'18]pentacosa-1(25),2,4,6,21,23-hexaen-12-yl]carbamate (1460301-50-1)

Guidance literature:

With sodium carbonate; In dichloromethane; water; at 0 ℃; for 2h;

Reference yield: 96.0%

benzyl N-[(12R,16S,18S)-16-amino-8,13-dioxo-20-oxa-9,14-diazatetracyclo[19.3.1.02,7.014,18]pentacosa-1(25),2,4,6,21,23-hexaen-12-yl]carbamate hydrochloride + phenyl chloroformate (1885-14-9) → benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.02'7.014'18]pentacosa-1(25),2,4,6,21,23-hexaen-12-yl]carbamate (1460301-50-1)

Guidance literature:

With sodium carbonate; In water; at 0 ℃; for 2h;

Reference yield: 96.0%

→ benzyl N-[(12R,16S,18S)-8,13-dioxo-16-[(phenoxycarbonyl)amino]-20-oxa-9,14-diazatetracyclo[19.3.1.02'7.014'18]pentacosa-1(25),2,4,6,21,23-hexaen-12-yl]carbamate (1460301-50-1)

Guidance literature:

With sodium carbonate; In dichloromethane; water; at 0 - 20 ℃;

upstream raw materials:

methyl 3’-hydroxybiphenyl-2-carboxylate

3’-hydroxybiphenyl-2-carboxylic acid

C₂₇H₃₂N₂O₇

C₄₂H₅₀N₄O₁₀

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