N-(2,6-Dichlorophenyl)prop-2-enamide

Base Information

• Chemical Name: N-(2,6-Dichlorophenyl)prop-2-enamide
• CAS No.: 37511-45-8
• Molecular Formula: C₉H₇Cl₂NO
• Molecular Weight: 216.067
• DSSTox Substance ID: DTXSID20547669
• Nikkaji Number: J2.399.834C
• Wikidata: Q82426022

Synonyms:N-(2,6-Dichlorophenyl)prop-2-enamide;37511-45-8;SCHEMBL14203835;DTXSID20547669;AKOS008098442;EN300-8051584;Z273451082

Chemical Property of N-(2,6-Dichlorophenyl)prop-2-enamide

Chemical Property:

• XLogP3: 1.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 214.9904692
• Heavy Atom Count: 13
• Complexity: 198

Purity/Quality:

N-(2,6-DICHLOROPHENYL)-2-PROPENAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C=CC(=O)NC1=C(C=CC=C1Cl)Cl

Technology Process of N-(2,6-Dichlorophenyl)prop-2-enamide

There total 1 articles about N-(2,6-Dichlorophenyl)prop-2-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acryloyl chloride (814-68-6,25189-84-8) + 2,6-Dichloroaniline (608-31-1) → N-2,6-dichlorophenyl-acrylamide (37511-45-8)

Guidance literature:

Reference yield: 80.0%

4-bromo-2-chloro-3-iodo-pyridine (916203-52-6) + N-2,6-dichlorophenyl-acrylamide (37511-45-8) → 5-chloro-1-(2,6-dichlorophenyl)-1,6-naphthyridin-2(1H)-one (916203-59-3)

Guidance literature:

With sodium acetate; potassium bromide; palladium diacetate; In various solvent(s); at 90 - 100 ℃;

DOI:10.1021/jo061618f

Reference yield: 76.0%

1-(2-pyridyl)piperazine (34803-66-2) + N-2,6-dichlorophenyl-acrylamide (37511-45-8) → N-(2,6-Dichloro-phenyl)-3-(4-pyridin-2-yl-piperazin-1-yl)-propionamide (86524-04-1)

Guidance literature:

In toluene; Heating;

DOI:10.1021/jm00384a002

upstream raw materials:

acryloyl chloride

2,6-Dichloroaniline

Downstream raw materials:

N-(2,6-Dichloro-phenyl)-3-(4-pyridin-2-yl-piperazin-1-yl)-propionamide

5-chloro-1-(2,6-dichlorophenyl)-1,6-naphthyridin-2(1H)-one

7-chloro-1-(2,6-dichlorophenyl)-5-(2,4-difluorophenyl)-1,6-naphthyridin-2-(1H)-one

1-(2,6-dichlorophenyl)-5-(2,4-difluorophenyl)-1,6-naphthyridin-2(1H)-one

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