(7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester

Base Information

Chemical Name:(7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester
CAS No.:197850-25-2
Molecular Formula:C₁₅H₁₄N₄O₃
Molecular Weight:298.301
Hs Code.:

Synonyms:(7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester

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Chemical Property of (7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester

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Technology Process of (7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester

There total 7 articles about (7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 192653-52-4
methyl 3-({[(methoxycarbonyl)amino][(methoxycarbonyl)imino]methyl}amino)-4-(phenylmethyl)-1H-pyrrole-2-carboxylate

: 197850-25-2
(7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester

Guidance literature:: With sodium methylate; for 2h; Ambient temperature;
DOI:10.1021/jo971062j

Reference yield:

: 56069-64-8
[E]-α-cyanocinnamaldehyde

: 197850-25-2
(7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 10percent Pd/C / methanol / 0.58 h / 2585.7 Torr

2: sodium acetate / H₂O / Ambient temperature

3: NaOMe / 1.) room temperature, 2 h, 2.) reflux, 30 min

4: 41 percent / AcOH / methanol / Ambient temperature

5: 76 percent / NaOMe / 2 h / Ambient temperature

With hydrogen; sodium methylate; sodium acetate; acetic acid; palladium on activated charcoal; In methanol; water;
DOI:10.1021/jo971062j

Reference yield:

: 100-52-7
benzaldehyde

: 197850-25-2
(7-Benzyl-4-oxo-4,5-dihydro-3H-pyrrolo[3,2-d]pyrimidin-2-yl)-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 68 percent / NaOMe / methanol / Ambient temperature

2: 100 percent / 6 N HCl / 0.5 h / Ambient temperature

3: H₂ / 10percent Pd/C / methanol / 0.58 h / 2585.7 Torr

4: sodium acetate / H₂O / Ambient temperature

5: NaOMe / 1.) room temperature, 2 h, 2.) reflux, 30 min

6: 41 percent / AcOH / methanol / Ambient temperature

7: 76 percent / NaOMe / 2 h / Ambient temperature

With hydrogenchloride; hydrogen; sodium methylate; sodium acetate; acetic acid; palladium on activated charcoal; In methanol; water;
DOI:10.1021/jo971062j