2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Base Information

Chemical Name:2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)
CAS No.:1598437-73-0
Molecular Formula:C₃₂H₁₀F₆N₂O₄S₄
Molecular Weight:728.697
Hs Code.:

Synonyms:2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

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Chemical Property of 2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

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Technology Process of 2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

There total 5 articles about 2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 1598437-72-9
2-bromo-5-(2,4,6-trifluorophenyl)-5H-thieno[2.3-c]pyrrole-4,6-dione

: 171290-94-1
5,5'-bis(tri-n-butylstannyl)-2,2'-bithiophene

: 1598437-73-0
2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; In 5,5-dimethyl-1,3-cyclohexadiene; for 6h; Inert atmosphere; Reflux;

Reference yield:

: 171290-94-1
5,5'-bis(tri-n-butylstannyl)-2,2'-bithiophene

: 1598437-73-0
2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Guidance literature:: With tetrakis(triphenylarsine)palladium⁽⁰⁾;

Reference yield:

: 6007-83-6
2,3-thiophenedicarboxylic acid anhydride

: 1598437-73-0
2,2'-(2,2'-bithiophene-5,5'-diyl)bis(5-(2,4,6-trifluorophenyl)-5H-thieno[2,3-c]pyrrole-4,6-dione)

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 24 h / Reflux

1.2: 3 h / Reflux

2.1: sulfuric acid; N-Bromosuccinimide; trifluoroacetic acid / 20 °C / Cooling with ice

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane / 5,5-dimethyl-1,3-cyclohexadiene / 6 h / Inert atmosphere; Reflux

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; N-Bromosuccinimide; triphenyl-arsane; sulfuric acid; trifluoroacetic acid; In 5,5-dimethyl-1,3-cyclohexadiene; toluene;