1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester

Base Information

Chemical Name:1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester
CAS No.:155219-87-7
Molecular Formula:C₁₈H₂₆N₂O₂Si
Molecular Weight:330.502
Hs Code.:

Synonyms:1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester

Suppliers and Price of 1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester

There total 3 articles about 1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 111097-70-2
(4-Iodo-but-2-ynyl)-trimethyl-silane

: 155219-78-6
1-benzyl-2-hydrazinecarboxylic acid allyl ester

: 155219-87-7
1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester

Guidance literature:: With potassium carbonate; lithium iodide; In acetone; for 18h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96267-2

Reference yield:

: 100-52-7
benzaldehyde

: 155219-87-7
1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / toluene / 18 h / Ambient temperature

2: 99 percent / pTSA, NaBH₃CN / tetrahydrofuran / 3.5 h / Ambient temperature

3: 81 percent / K₂CO₃, LiI / acetone / 18 h / Ambient temperature

With sodium cyanoborohydride; potassium carbonate; toluene-4-sulfonic acid; lithium iodide; In tetrahydrofuran; acetone; toluene;
DOI:10.1016/S0040-4020(01)96267-2

Reference yield:

: N'-[1-Phenyl-meth-(E)-ylidene]-hydrazinecarboxylic acid allyl ester

: 155219-87-7
1-benzyl-1-<4-(trimethylsilyl)-2-butenyl>-2-hydrazinecarboxylic acid allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / pTSA, NaBH₃CN / tetrahydrofuran / 3.5 h / Ambient temperature

2: 81 percent / K₂CO₃, LiI / acetone / 18 h / Ambient temperature

With sodium cyanoborohydride; potassium carbonate; toluene-4-sulfonic acid; lithium iodide; In tetrahydrofuran; acetone;
DOI:10.1016/S0040-4020(01)96267-2