4-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)-phenyl]-[2,2']bipyridinyl

Base Information

Chemical Name:4-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)-phenyl]-[2,2']bipyridinyl
CAS No.:858098-81-4
Molecular Formula:C₂₈H₂₇BN₂O₂
Molecular Weight:434.346
Hs Code.:

Synonyms:4-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)-phenyl]-[2,2']bipyridinyl

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Chemical Property of 4-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)-phenyl]-[2,2']bipyridinyl

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Technology Process of 4-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)-phenyl]-[2,2']bipyridinyl

There total 1 articles about 4-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)-phenyl]-[2,2']bipyridinyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 858098-80-3
N₂C₁₀H₇C₆H₄C₆H₄Br

: 73183-34-3
bis(pinacol)diborane

: 858098-81-4
4-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)-phenyl]-[2,2']bipyridinyl

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In dimethyl sulfoxide; under Ar atm. to soln. bpy-Ph-Br, K2CO3, and bis(pinacolato)diboron in DMSO PdCl2(dppf) was added and heated to 105°C for 25 h; react. mixt. was cooled to room temp., water was added, extd. with CH2Cl2, org. phase was evapd. in vacuo, hexane was added;
DOI:10.1021/ic0483141