(S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride

Base Information

• Chemical Name: (S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride
• CAS No.: 1221568-17-7
• Molecular Formula: C₂₀H₁₈ClN₃O₃
• Molecular Weight: 383.834

Synonyms:(S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride

Chemical Property of (S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride

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Technology Process of (S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride

There total 1 articles about (S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.7%

(S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoic acid (1221568-16-6) → (S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride (1221568-17-7)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.bmc.2010.01.008

Reference yield: 68.1%

(S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride (1221568-17-7) + diethylamine (109-89-7) → (S)-N,N-diethyl-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanamide (1221568-31-5)

Guidance literature:

With potassium tert-butylate; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.bmc.2010.01.008

Reference yield: 67.1%

methyl 6-aminohexanoate hydrochloride (2780-89-4) + (S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoyl chloride (1221568-17-7) → (S)-methyl 6-(2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanamido)hexanoate (1221568-35-9)

Guidance literature:

With potassium tert-butylate; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.bmc.2010.01.008

upstream raw materials:

(S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanoic acid

Downstream raw materials:

(S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenyl-N-(pyridin-3-yl)propanamide

(S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenyl-N-propylpropanamide

methyl 4-((S)-2-(2-(3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanamido)-4-(methylthio)butanoate

(S)-N-(3-chloro-4-fluorophenyl)-2-((3-methyl-2-oxoquinoxalin-1(2H)-yl)acetamido)-3-phenylpropanamide

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