C₅₂H₇₈N₈O₆Si

Base Information

• Chemical Name: C₅₂H₇₈N₈O₆Si
• CAS No.: 1009094-34-1
• Molecular Formula: C₅₂H₇₈N₈O₆Si
• Molecular Weight: 939.327
• Mol file: 1009094-34-1.mol

Synonyms:C₅₂H₇₈N₈O₆Si

Chemical Property of C₅₂H₇₈N₈O₆Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₂H₇₈N₈O₆Si

There total 12 articles about C₅₂H₇₈N₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

C41H62N6O7Si (1009094-33-0) + N-[(2S)-2-amino-3-phenylpropyl]-N,N-dimethylamine (29802-26-4) → C52H78N8O6Si (1009094-34-1)

Guidance literature:

C₄₁H₆₂N₆O₇Si; With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; at 20 ℃; for 0.166667h;

N-[(2S)-2-amino-3-phenylpropyl]-N,N-dimethylamine; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

C12H14BrNO4 (1009091-84-2) → C52H78N8O6Si (1009094-34-1)

Guidance literature:

Multi-step reaction with 5 steps

1.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

1.2: 1 h

2.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

3.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

3.2: 2 h

3.3: 5 h

4.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h

4.2: 1 h / 70 °C

5.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 0.17 h / 20 °C

5.2: 2 h / 20 °C

With titanium(IV) isopropylate; potassium acetate; diisobutylaluminium hydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; toluene;

Reference yield:

C9H10BrNO2 → C52H78N8O6Si (1009094-34-1)

Guidance literature:

Multi-step reaction with 7 steps

1.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 16 h / pH 2

1.2: pH 7 / Alkaline aqueous solution

2.1: benzene / Heating / reflux

3.1: titanium(IV) isopropylate / toluene / 0.17 h / 120 °C / Microwave irradiation

3.2: 1 h

4.1: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

5.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 2 h / 0 °C

5.2: 2 h

5.3: 5 h

6.1: potassium acetate; caesium carbonate / dimethyl sulfoxide / 0.17 h

6.2: 1 h / 70 °C

7.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 0.17 h / 20 °C

7.2: 2 h / 20 °C

With titanium(IV) isopropylate; hydrogenchloride; methyl orange; potassium acetate; diisobutylaluminium hydride; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; pyridine hydrogenfluoride; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; benzene;

upstream raw materials:

C₄₁H₆₂N₆O₇Si

N-[(2S)-2-amino-3-phenylpropyl]-N,N-dimethylamine

C₉H₁₂BrNO₂

C₈H₁₀BNO₄

Downstream raw materials:

C₄₆H₆₆N₆O₆

C₄₆H₆₄N₈O₆