1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene

Base Information

Chemical Name:1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene
CAS No.:1616280-55-7
Molecular Formula:C₁₉H₁₃FINO₆S
Molecular Weight:529.284
Hs Code.:

Synonyms:1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene

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Chemical Property of 1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene

Chemical Property:

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Technology Process of 1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene

There total 5 articles about 1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616280-52-4
5-fluoro-4-(2-fluorophenoxy)-2-nitroaniline

: 1616280-55-7
1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / acetonitrile; water / 0.5 h / 0 °C

1.2: 1 h

2.1: potassium carbonate / acetonitrile / 1 h / 80 °C

With hydrogenchloride; potassium carbonate; sodium nitrite; In water; acetonitrile;

Reference yield:

: 946699-01-0
3-fluoro-4-(2-fluorophenoxy)aniline

: 1616280-55-7
1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium nitrate; trifluoroacetic anhydride / 2 h

2.1: sodium nitrite; hydrogenchloride / acetonitrile; water / 0.5 h / 0 °C

2.2: 1 h

3.1: potassium carbonate / acetonitrile / 1 h / 80 °C

With hydrogenchloride; potassium carbonate; potassium nitrate; trifluoroacetic anhydride; sodium nitrite; In water; acetonitrile;

Reference yield:

: 367-12-4
2-fluorophenol

: 1616280-55-7
1-(2-fluorophenoxy)-4-iodo-2-[4-(methylsulfonyl)phenoxy]-5-nitrobenzene

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / acetonitrile / 1 h / 80 °C

2.1: ammonium chloride; iron / water; isopropyl alcohol / 1 h / 60 °C

3.1: potassium nitrate; trifluoroacetic anhydride / 2 h

4.1: sodium nitrite; hydrogenchloride / acetonitrile; water / 0.5 h / 0 °C

4.2: 1 h

5.1: potassium carbonate / acetonitrile / 1 h / 80 °C

With hydrogenchloride; iron; potassium carbonate; ammonium chloride; potassium nitrate; trifluoroacetic anhydride; sodium nitrite; In water; isopropyl alcohol; acetonitrile;