4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol]

Base Information

Chemical Name:4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol]
CAS No.:1309660-16-9
Molecular Formula:C₃₃H₃₂N₄O₄
Molecular Weight:548.641
Hs Code.:

Synonyms:4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol]

Chemical Property:

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Technology Process of 4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol]

There total 4 articles about 4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1174233-50-1
C₃₃H₂₈O₆

: 1309660-16-9
4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol]

Guidance literature:: With hydrazine hydrate; at 150 ℃; for 0.0333333h; Microwave irradiation;
DOI:10.1016/j.ejmech.2011.03.028

Reference yield:

: 90-02-8
salicylaldehyde

: 1309660-16-9
4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol]

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid

2: potassium hydroxide / ethanol

3: hydrazine hydrate / 0.03 h / 150 °C / Microwave irradiation

With sulfuric acid; hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1016/j.ejmech.2011.03.028

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1309660-16-9
4,4'-methylenebis[2-(3-(4-methoxyphenyl)-4,5-dihydro-1H-pyrazol-5-yl)phenol]

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol

2: hydrazine hydrate / 0.03 h / 150 °C / Microwave irradiation

With hydrazine hydrate; potassium hydroxide; In ethanol;
DOI:10.1016/j.ejmech.2011.03.028