tricarbonyl(η6-8,8-dimethylheptafulvene)chromium(0)

Base Information

Chemical Name:tricarbonyl(η6-8,8-dimethylheptafulvene)chromium(0)
CAS No.:38814-48-1
Molecular Formula:C₁₃H₁₂CrO₃
Molecular Weight:268.232
Hs Code.:

Synonyms:tricarbonyl(η6-8,8-dimethylheptafulvene)chromium(0)

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Chemical Property of tricarbonyl(η6-8,8-dimethylheptafulvene)chromium(0)

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Technology Process of tricarbonyl(η6-8,8-dimethylheptafulvene)chromium(0)

There total 1 articles about tricarbonyl(η6-8,8-dimethylheptafulvene)chromium(0) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 96093-48-0,88031-74-7
dicarbonyl(2-6:2'-4'-η-[1-(2,3-dimethyl-3-butene-1,2-diyl)-7-isopropylidene-3,5-cycloheptadiene-2-yl])chromium

: 38814-48-1
tricarbonyl(η6-8,8-dimethylheptafulvene)chromium(0)

: 513-81-5
2,3-dimethyl-buta-1,3-diene

Guidance literature:: In not given; on heating;
DOI:10.1016/0022-328X(83)80064-3

Reference yield: 41.0%

: 38814-48-1
tricarbonyl[1-6-η(8,8-dimethylheptafulvene)]chromium(O)

: 2175-90-8
6,6-Diphenylfulvene

: 89234-41-3
dicarbonyl(1''-5'':3'-5'-η-[(cyclopentadiendiyl)(7-isopropyliden-1,4-cycloheptadien-3,6-diyl)diphenylmethane])chromium

Guidance literature:: In hexane; Irradiation (UV/VIS); under N2 Cr(CO)3C10H12 and 6,6-diphenylfulvene in n-hexane was irradiated with dived Hg lamp for 75 min at 263 K; filtrated, concd.; chromy on SiO2 with n-hexane/CHCl3 (3:1); the first two zones contain educts; from the third zone solvent evapd., solved in n-hexane/toluene (1:1) and cooled to 253 K crystn.;

Reference yield: 32.0%

: 38814-48-1
tricarbonyl[1-6-η(8,8-dimethylheptafulvene)]chromium(O)

: 2320-32-3
6-methyl-6-phenylfulvene

: 89300-34-5,89215-76-9,89301-36-0,89215-63-4
dicarbonyl(1''-5'':3',5',-η-[1-(cyclopentadiendiyl)-1-(7-isopropyliden-1,4-cycloheptadien-3,6-diyl)-1-phenylethane])chromium

Guidance literature:: In hexane; Irradiation (UV/VIS); under N2 soln. of Cr(CO)3C10H12 and 6-methyl-6-phenyl-fulvene in n-hexane for 30 min with a dived Hg lamp irradiated at 263 K; filtrated, concd.;; chromy on Al2O3 with n-hexane; in the 1st and 2nd zone educts; the 3rd zone was divided for 5 fractions; in the first 3 of them was present theCr(CO)2C16H16CH3C6H5; crystn.by cooling of the concd. soln.; elem. anal.;