2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene

Base Information

Chemical Name:2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene
CAS No.:1093262-48-6
Molecular Formula:C₁₃H₇BrCl₂F₂O
Molecular Weight:368.005
Hs Code.:

Synonyms:2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene

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Chemical Property of 2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene

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Technology Process of 2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene

There total 1 articles about 2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 261762-91-8
6-chloro-2-fluoro-3-methylphenol

: 176673-72-6
5-bromo-2-chloro-1,3-difluoro-benzene

: 1093262-48-6
2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene

Guidance literature:: 6-chloro-2-fluoro-3-methylphenol; With 18-crown-6 ether; potassium tert-butylate; In tetrahydrofuran; dimethyl sulfoxide; at 20 ℃; for 0.25h;

5-bromo-2-chloro-1,3-difluoro-benzene; In tetrahydrofuran; dimethyl sulfoxide; at 130 ℃; for 72h;

Reference yield: 62.4%

: 1093262-48-6
2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene

: 1093262-50-0
2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-4-(bromomethyl)-1-chloro-3-fluorobenzene

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; for 16h; Reflux;

Reference yield:

: 1093262-48-6
2-[(5-bromo-2-chloro-3-fluorophenyl)oxy]-1-chloro-3-fluoro-4-methylbenzene

: 1093262-56-6
3-{[3-(aminomethyl)-6-chloro-2-fluorophenyl]oxy}-4-chloro-5-fluorobenzonitrile

Guidance literature:: Multi-step reaction with 4 steps

1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 16 h / Reflux

2: sodium azide / dimethyl sulfoxide / 72 h / 25 °C

3: water; triphenylphosphine / tetrahydrofuran / 48 h / 25 °C

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 0.42 h / 120 °C / Inert atmosphere; Microwave irradiation

With N-Bromosuccinimide; sodium azide; 2,2'-azobis(isobutyronitrile); water; triphenylphosphine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; tetrachloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;