C₁₉H₂₇NO₃Si

Base Information

Chemical Name:C₁₉H₂₇NO₃Si
CAS No.:1367352-96-2
Molecular Formula:C₁₉H₂₇NO₃Si
Molecular Weight:345.514
Hs Code.:

C<sub>19</sub>H<sub>27</sub>NO<sub>3</sub>Si

Synonyms:C₁₉H₂₇NO₃Si

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Chemical Property of C₁₉H₂₇NO₃Si

Chemical Property:

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Technology Process of C₁₉H₂₇NO₃Si

There total 8 articles about C₁₉H₂₇NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1367352-94-0
C₁₉H₂₉NO₃Si

: 1367352-96-2
C₁₉H₂₇NO₃Si

Guidance literature:: With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile; at -10 - -5 ℃; for 2h;
DOI:10.1016/j.tetlet.2012.01.098

Reference yield:

: 15761-39-4,59433-50-0
1-(tert-butoxycarbonyl)-L-proline

: 1367352-96-2
C₁₉H₂₇NO₃Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / 0 - 20 °C

1.2: 22 h / 50 °C

2.1: triethylamine / tetrahydrofuran / 4 h / -65 - -40 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water / 0.67 h / 0 - 60 °C

4.1: platinum(IV) oxide; hydrogen / methanol; ethyl acetate / 6 h / 20 °C

5.1: water; trifluoroacetic acid / dichloromethane / 2 h

6.1: ammonia / water / 0.67 h / 75 °C / sealed tube

7.1: pyridine; silver nitrate / tetrahydrofuran / 5 h / 20 °C

8.1: N,N,N,N,N,N-hexamethylphosphoric triamide; oxygen; lithium diisopropyl amide; phosphorous acid trimethyl ester / tetrahydrofuran / 4 h / -75 - -65 °C

9.1: sodium periodate; ruthenium trichloride / tetrachloromethane; water; acetonitrile / 2 h / -10 - -5 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; platinum(IV) oxide; ruthenium trichloride; sodium periodate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; ammonia; water; hydrogen; oxygen; sodium carbonate; silver nitrate; triethylamine; 1,1'-carbonyldiimidazole; trifluoroacetic acid; lithium diisopropyl amide; phosphorous acid trimethyl ester; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water; ethyl acetate; acetonitrile; 3.1: Suzuki coupling;
DOI:10.1016/j.tetlet.2012.01.098

Reference yield:

: 1367352-83-7
C₂₀H₂₇NO₅

: 1367352-96-2
C₁₉H₂₇NO₃Si

Guidance literature:: Multi-step reaction with 6 steps

1: platinum(IV) oxide; hydrogen / methanol; ethyl acetate / 6 h / 20 °C

2: water; trifluoroacetic acid / dichloromethane / 2 h

3: ammonia / water / 0.67 h / 75 °C / sealed tube

4: pyridine; silver nitrate / tetrahydrofuran / 5 h / 20 °C

5: N,N,N,N,N,N-hexamethylphosphoric triamide; oxygen; lithium diisopropyl amide; phosphorous acid trimethyl ester / tetrahydrofuran / 4 h / -75 - -65 °C

6: sodium periodate; ruthenium trichloride / tetrachloromethane; water; acetonitrile / 2 h / -10 - -5 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; platinum(IV) oxide; ruthenium trichloride; sodium periodate; ammonia; water; hydrogen; oxygen; silver nitrate; trifluoroacetic acid; lithium diisopropyl amide; phosphorous acid trimethyl ester; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetlet.2012.01.098