2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester

Base Information

Chemical Name:2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester
CAS No.:197314-04-8
Molecular Formula:C₁₈H₁₈O₂S₂
Molecular Weight:330.472
Hs Code.:

2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid <i>S</i>-methyl ester

Synonyms:2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester

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Technology Process of 2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester

There total 1 articles about 2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 77-78-1
dimethyl sulfate

: 195305-64-7
(3-Benzoyl-phenyl)-bis-methylsulfanyl-thioacetic acid S-methyl ester

: 197314-04-8
2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester

Guidance literature:: (3-Benzoyl-phenyl)-bis-methylsulfanyl-thioacetic acid S-methyl ester; With potassium tert-butylate; In tetrahydrofuran; at 20 - 25 ℃; for 0.166667h;

dimethyl sulfate; In tetrahydrofuran; at 20 - 25 ℃; for 0.5h;
DOI:10.1055/s-2002-28521

Reference yield: 94.0%

: 197314-04-8
2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester

: 197314-10-6
2-(3-benzoyl-phenyl)-thiopropionic acid S-methyl ester

Guidance literature:: With mesna; In acetonitrile; at 20 - 25 ℃; for 1h;
DOI:10.1055/s-2002-28521

Reference yield:

: 197314-04-8
2-(3-benzoyl-phenyl)-2-methylsulfanyl-thiopropionic acid S-methyl ester

: 22071-15-4,22161-86-0
ketoprofen

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / MeSNa / acetonitrile / 1 h / 20 - 25 °C

2: 100 percent / aq. KOH / acetone / 2 h / Heating

With potassium hydroxide; mesna; In acetone; acetonitrile;
DOI:10.1055/s-2002-28521