[(η⁶-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl

Base Information

• Chemical Name: [(η⁶-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl
• CAS No.: 1446756-42-8
• Molecular Formula: C₄₁H₄₇ClN₃O₃P₂RuS*Cl
• Molecular Weight: 895.832

Synonyms:[(η⁶-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl

Chemical Property of [(η⁶-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl

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Technology Process of [(η⁶-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl

There total 4 articles about [(η⁶-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + C18H14O3PS(1-)*C13H19N3P(1+) (1446756-37-1) → [(η6-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl (1446756-42-8)

Guidance literature:

In methanol; for 10h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1016/j.poly.2013.05.008

Reference yield: 76.0%

[(η6-p-cymene)RuCl2(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)]Cl (1065225-20-8) + sodium 3-(diphenylphosphanyl)benzenesulfonate (63995-75-5) → [(η6-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl (1446756-42-8)

Guidance literature:

In methanol; for 10h; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1016/j.poly.2013.05.008

Reference yield:

[(η6-p-cymene)RuCl2(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)](mtppms) (1446756-42-8) → [(η6-p-cymene)RuCl(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)(mtppms)]Cl (1446756-42-8)

Guidance literature:

In methanol; Inert atmosphere; Schlenk technique; Reflux;

DOI:10.1016/j.poly.2013.05.008

upstream raw materials:

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

C₁₈H₁₄O₃PS^(1-)*C₁₃H₁₉N₃P⁽¹⁺⁾

[(η⁶-p-cymene)RuCl₂(1-benzyl-1-azonia-3,5-diaza-7-phosphaadamantyl)]Cl

sodium 3-(diphenylphosphanyl)benzenesulfonate

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