N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide

Base Information

Chemical Name:N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide
CAS No.:1620727-18-5
Molecular Formula:C₂₉H₃₀ClN₃O₃S
Molecular Weight:536.094
Hs Code.:

Synonyms:N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide

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Chemical Property of N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide

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Technology Process of N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide

There total 4 articles about N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1620727-53-8
3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)aniline

: 141-75-3
butyryl chloride

: 1620727-18-5
N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide

Guidance literature:: 3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)aniline; With triethylamine; In dichloromethane; at 0 ℃; for 0.166667h;

butyryl chloride; In dichloromethane; for 3h;
DOI:10.3390/molecules19022694

Reference yield:

: 100643-71-8
descarboethoxyloratadine

: 1620727-18-5
N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C

1.2: 2 h

2.1: hydrogenchloride; tin(ll) chloride / ethanol / Reflux

3.1: triethylamine / dichloromethane / 0.17 h / 0 °C

3.2: 3 h

With hydrogenchloride; triethylamine; tin(ll) chloride; In ethanol; dichloromethane;
DOI:10.3390/molecules19022694

Reference yield:

: 121-51-7
3-nitrobenzenesulphonyl chloride

: 1620727-18-5
N-(3-((4-(8-Chloro-5H-benzo[5,6]cyclohepta[1,2-b]pyridin-11(6H)-ylidene)piperidin-1-yl)sulfonyl)phenyl)butyramide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.17 h / 0 °C

1.2: 2 h

2.1: hydrogenchloride; tin(ll) chloride / ethanol / Reflux

3.1: triethylamine / dichloromethane / 0.17 h / 0 °C

3.2: 3 h

With hydrogenchloride; triethylamine; tin(ll) chloride; In ethanol; dichloromethane;
DOI:10.3390/molecules19022694