(R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol

Base Information

Chemical Name:(R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol
CAS No.:1352816-34-2
Molecular Formula:C₈H₁₄O₃
Molecular Weight:158.197
Hs Code.:

Synonyms:(R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol

Suppliers and Price of (R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol

Chemical Property:

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Technology Process of (R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol

There total 1 articles about (R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3413-44-3
(R)-2-cyclohexen-1-ol

: 1352816-34-2
(R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2.1: oxygen / dichloromethane / 0.5 h / -78 °C

2.2: 2 h / -78 - 0 °C

3.1: dibenzylammonium trifluoroacetate salt / dichloromethane / 17 h / 0 - 20 °C

4.1: sodium tetrahydroborate / methanol / 1 h / 0 °C

With sodium tetrahydroborate; oxygen; N-ethyl-N,N-diisopropylamine; dibenzylammonium trifluoroacetate salt; In methanol; dichloromethane;
DOI:10.1002/anie.201104681

Reference yield: 86.0%

: 1352816-34-2
(R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol

: 98-59-9
p-toluenesulfonyl chloride

: 1352816-04-6
C₁₅H₂₀O₅S

Guidance literature:: With sodium hydride; In toluene; paraffin oil; for 24h; Cooling;
DOI:10.1002/anie.201104681

Reference yield:

: 1352816-34-2
(R)-(3-(methoxymethoxy)cyclopent-1-enyl)methanol

: 1352816-05-7
C₄₇H₆₀O₈Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / toluene; paraffin oil / 24 h / Cooling

2.1: potassium hexamethylsilazane / tetrahydrofuran / 1 h / -40 - -20 °C

2.2: 0.08 h / -20 °C

2.3: 0.83 h / -20 - 0 °C

With potassium hexamethylsilazane; sodium hydride; In tetrahydrofuran; toluene; paraffin oil;
DOI:10.1002/anie.201104681