C₃₀H₄₀O₇

Base Information

Chemical Name:C₃₀H₄₀O₇
CAS No.:259258-00-9
Molecular Formula:C₃₀H₄₀O₇
Molecular Weight:512.643
Hs Code.:

C<sub>30</sub>H<sub>40</sub>O<sub>7</sub>

Synonyms:C₃₀H₄₀O₇

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Chemical Property of C₃₀H₄₀O₇

Chemical Property:

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Technology Process of C₃₀H₄₀O₇

There total 15 articles about C₃₀H₄₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 157220-24-1
C₄₁H₆₄O₈Si

: 259258-00-9
C₃₀H₄₀O₇

Guidance literature:: With dimethylsulfide; boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 0.333333h;
DOI:10.1021/jo990988j

Reference yield:

: 100-39-0
benzyl bromide

: 259258-00-9
C₃₀H₄₀O₇

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / sodium hydride / tetrahydrofuran; dimethylformamide; various solvent(s) / 0 - 50 °C

2: 77 percent / dimethyl sulfide; BF₃*Et₂O / CH₂Cl₂ / 0.33 h / 0 °C

With dimethylsulfide; boron trifluoride diethyl etherate; sodium hydride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: Etherification / 2: Hydrolysis;
DOI:10.1021/jo990988j

Reference yield:

: (3R,3aR,5S,6R,7S,8S,8aS)-8-Benzyloxy-5-methoxymethoxymethyl-3,7-dimethyl-6-triisopropylsilanyloxy-octahydro-furo[3,2-b]oxepin-2-ol

: 259258-00-9
C₃₀H₄₀O₇

Guidance literature:: Multi-step reaction with 12 steps

1.1: NaHMDS / tetrahydrofuran / 0.5 h / 0 °C

1.2: 71 percent / tetrahydrofuran / 0 - 20 °C

2.1: 98 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 2.5 h / 20 °C

3.1: 9-borabicyclo[3.3.1]nonane / tetrahydrofuran / 0 - 20 °C

3.2: 9.90 g / hydrogen peroxide; sodium hydroxide / tetrahydrofuran / 1.5 h / 20 °C

4.1: triethylamine; SO₃*pyridine / CH₂Cl₂; dimethylsulfoxide / 0.5 h / 0 °C

5.1: acetic acid / tetrahydrofuran; H₂O / 20 °C

6.1: 6.98 g / pyridinium dichromate; molecular sieves 4A / CH₂Cl₂ / 2 h / 20 °C

7.1: LiHMDS / tetrahydrofuran; hexane / 0.5 h / -78 °C

7.2: 92 percent / tetrahydrofuran; hexane / -78 - 0 °C

8.1: 79 percent / tetrahydrofuran; diethyl ether / 0.75 h / -78 °C

9.1: N,N'-bis(2,4,6-Me₃C₆H₂CH₂)-(S,S)-1,2-Ph₂-1,2-diaminoethane; osmium tetroxide / CH₂Cl₂ / 2 h / -90 °C

9.2: 85 percent / NaHSO₃ / tetrahydrofuran; H₂O / 2 h / Heating

10.1: 86 percent / camphorsulfonic acid / benzene / 36 h / 20 °C

11.1: 83 percent / sodium hydride / tetrahydrofuran; dimethylformamide; various solvent(s) / 0 - 50 °C

12.1: 77 percent / dimethyl sulfide; BF₃*Et₂O / CH₂Cl₂ / 0.33 h / 0 °C

With osmium(VIII) oxide; dipyridinium dichromate; pyridine-SO₃ complex; dimethylsulfide; 4 A molecular sieve; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; sodium hydride; acetic acid; (1S,2S)-1,2-diphenyl-N¹,N²-bis(mesitylmethyl)ethane-1,2-diamine; triethylamine; 9-bora-bicyclo[3.3.1]nonane; lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; benzene; 1.1: Dehydrobromination / 1.2: methylenation; Wittig reaction / 2.1: Addition / 3.1: hydroboration / 3.2: Oxidation / 4.1: Oxidation / 5.1: Hydrolysis / 6.1: Oxidation / 7.1: Metallation / 7.2: Methylation / 8.1: Addition / 9.1: Oxidation / 9.2: Ring cleavage / 10.1: Cyclization / 11.1: Etherification / 12.1: Hydrolysis;
DOI:10.1021/jo990988j