2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine

Base Information

Chemical Name:2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine
CAS No.:851340-66-4
Molecular Formula:C₂₈H₂₄N₆O₃
Molecular Weight:492.537
Hs Code.:

Synonyms:2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine

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Chemical Property of 2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine

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Technology Process of 2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine

There total 5 articles about 2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 851340-85-7
2-(2'-benzyloxy-4'-cyanobiphenyl-4-yl)-1H-benzimidazole-5-carbonitrile

: 851340-66-4
2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine

Guidance literature:: With hydroxylamine hydrochloride; potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃;
DOI:10.1016/j.bmc.2005.07.024

Reference yield: 90.0%

: 851340-66-4
2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine

Guidance literature:

Reference yield:

: 87199-17-5
4-formylphenylboronic acid,

: 851340-66-4
2-[2'-benzyloxy-4'-(N-hydroxyamidino)biphenyl-4-yl]-1H-benzimidazole-5-N-hydroxyamidine

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / Na₂CO₃ / tetrakis(triphenylphosphine)palladium / toluene; H₂O; methanol / 12 h / 80 °C

2: 75 percent / sodium hydrogen sulfite / dimethylformamide / Heating

3: 90 percent / hydroxylamine hydrochloride; potassium t-butoxide / dimethylsulfoxide / 20 °C

With hydroxylamine hydrochloride; potassium tert-butylate; sodium carbonate; sodium hydrogensulfite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 1: Suzuki coupling;
DOI:10.1016/j.bmc.2005.07.024