2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate

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Chemical Name:2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate
CAS No.:1439358-84-5
Molecular Formula:C₂₆H₂₃BrN₂O₆
Molecular Weight:539.382
Hs Code.:

Synonyms:2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate

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Chemical Property of 2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate

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Technology Process of 2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate

There total 1 articles about 2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1439358-81-2
2-cyanoethyl 2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-1H-indeno[1,2-b]pyridine-3-carboxylate

: 1439358-84-5
2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate

Guidance literature:: With N-Bromosuccinimide; In methanol; at 10 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.060

Reference yield: 85.0%

: 1439358-84-5
2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate

: 1439358-81-2
2-cyanoethyl 2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4,5-dihydro-1H-indeno[1,2-b]pyridine-3-carboxylate

Guidance literature:: 2-cyanoethyl 4a-bromo-2-methyl-5-oxo-4-(3,4,5-trimethoxyphenyl)-4a,5-dihydroindeno[1,2-b]pyridine-3-carboxylate; With sodium hydroxide; In water; acetone; at 20 ℃; for 0.0333333h;

With hydrogenchloride; In water; acetone; pH=4 - 5;
DOI:10.1016/j.tet.2013.04.060