Technology Process of N-tert-butoxy-3-(4-trimethylstannanylphenoxy)propionamide
There total 4 articles about N-tert-butoxy-3-(4-trimethylstannanylphenoxy)propionamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0);
In
toluene;
at 20 ℃;
for 1.66667h;
Inert atmosphere;
Reflux;
DOI:10.1016/j.bmcl.2012.05.032
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium tert-butylate / tetrahydrofuran / 23 h / 20 °C
2: thionyl chloride / 1 h / Reflux
3: sodium carbonate / dichloromethane; water; diethyl ether / 5 h / 20 °C / Inert atmosphere
4: tetrakis(triphenylphosphine) palladium(0) / toluene / 1.67 h / 20 °C / Inert atmosphere; Reflux
With
tetrakis(triphenylphosphine) palladium(0); thionyl chloride; potassium tert-butylate; sodium carbonate;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; toluene;
DOI:10.1016/j.bmcl.2012.05.032
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate / dichloromethane; water; diethyl ether / 5 h / 20 °C / Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0) / toluene / 1.67 h / 20 °C / Inert atmosphere; Reflux
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
diethyl ether; dichloromethane; water; toluene;
DOI:10.1016/j.bmcl.2012.05.032
