1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone

Base Information

Chemical Name:1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone
CAS No.:303041-55-6
Molecular Formula:C₁₉H₂₀N₂O₇
Molecular Weight:388.377
Hs Code.:

Synonyms:1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone

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Chemical Property of 1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone

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Technology Process of 1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone

There total 4 articles about 1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 23583-55-3
1-(2-O-acetyl3,5-O-dibenzoyl-β-D-ribofuranosyl)-4-methoxy-2-pyrimidone

: 303041-55-6
1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone

Guidance literature:: With magnesium(II) perchlorate; 3,6,9-trimethyl-9H-carbazole; In water; isopropyl alcohol; Photolysis;
DOI:10.1021/jo0003652

Reference yield:

: 22224-41-5
1,3,5-tri-O-benzoyl-α-D-ribofuranoside

: 303041-55-6
1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / 2,6-lutidine / CH₂Cl₂ / 10 h / 20 °C

2: 83 percent / SnCl₄ / acetonitrile / 20 °C

3: 55 percent / 3,6-dimethyl-9-methylcarbazole; Mg(ClO₄)2 / propan-2-ol; H₂O / Photolysis

With 2,6-dimethylpyridine; magnesium(II) perchlorate; tin(IV) chloride; 3,6,9-trimethyl-9H-carbazole; In dichloromethane; water; isopropyl alcohol; acetonitrile; 1: Acylation / 2: Substitution / 3: Elimination;
DOI:10.1021/jo0003652

Reference yield:

: 22224-42-6
α-D-2-O-acetyl-1,3,5-tri-O-benzoylribofuranoside

: 303041-55-6
1-(2-O-acetyl-5-O-benzoyl-3-deoxy-β-D-erythro-pentofuranosyl)-4-methoxy-2-pyrimidone

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / SnCl₄ / acetonitrile / 20 °C

2: 55 percent / 3,6-dimethyl-9-methylcarbazole; Mg(ClO₄)2 / propan-2-ol; H₂O / Photolysis

With magnesium(II) perchlorate; tin(IV) chloride; 3,6,9-trimethyl-9H-carbazole; In water; isopropyl alcohol; acetonitrile; 1: Substitution / 2: Elimination;
DOI:10.1021/jo0003652