2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol

Base Information

Chemical Name:2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol
CAS No.:166193-90-4
Molecular Formula:C₄₁H₅₇NO₃Si₂
Molecular Weight:668.079
Hs Code.:

2-<<N-methyl-N-<4-(tert-butyldiphenylsilyl)oxy>butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol

Synonyms:2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol

Chemical Property:

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Technology Process of 2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol

There total 5 articles about 2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 166193-88-0
N-<4-<(tert-butyldiphenylsilyl)oxy>butyl>-2-<2-<(tert-butyldiphenylsilyl)oxy>ethyl>-2-oxazolidinone

: 166193-90-4
2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2.5h;
DOI:10.1021/jm00014a023

Reference yield:

: 130372-07-5
4-(tret-butyldiphenylsilyloxy)butan-1-ol

: 166193-90-4
2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / triphenoxymethylphosphonium iodide / CH₂Cl₂ / -68 - 20 °C

2: 1.) KH, 2.) 18-crown-6 / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, overnight

3: 60 percent / LiAlH₄ / tetrahydrofuran / 2.5 h / 0 °C

With lithium aluminium tetrahydride; 18-crown-6 ether; methyltriphenoxyphosphonium iodide; potassium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm00014a023

Reference yield:

: 149365-02-6
4-[(tert-butyldiphenylsilyl)oxy]-1-iodobutane

: 166193-90-4
2-<butyl>amino>-4-<(tert-butyldiphenylsilyl)oxy>-1,4-butanediol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) KH, 2.) 18-crown-6 / 1.) THF, 0 deg C, 30 min, 2.) THF, RT, overnight

2: 60 percent / LiAlH₄ / tetrahydrofuran / 2.5 h / 0 °C

With lithium aluminium tetrahydride; 18-crown-6 ether; potassium hydride; In tetrahydrofuran;
DOI:10.1021/jm00014a023