1-Butanol, 4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-

Base Information

• Chemical Name: 1-Butanol, 4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-
• CAS No.: 130372-07-5
• Molecular Formula: C20H28O2Si
• Molecular Weight: 328.527
• DSSTox Substance ID: DTXSID60435091
• Nikkaji Number: J896.003H
• Mol file: 130372-07-5.mol

Synonyms:130372-07-5;1-Butanol, 4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-;4-{[tert-butyl(diphenyl)silyl]oxy}butan-1-ol;4-(tert-butyldiphenylsiloxy)-1-butanol;4-((tert-Butyldiphenylsilyl)oxy)butan-1-ol;4-[tert-butyl(diphenyl)silyl]oxybutan-1-ol;SCHEMBL639531;DTXSID60435091;WGBBKMOBGARXLF-UHFFFAOYSA-N;4-(t-butyldiphenylsilyloxy)-butane-1-ol;4-(t-butyldiphenylsilyloxyl)-butan-1-ol;4-(tert-butyidiphenylsilyloxy)butan-1-ol;4-(tert-butyldiphenylsilyloxy)butan-1-ol;FT-0708462;4-(tert-butyl-diphenyl-silanyloxy)-butan-1-ol;A1-22931

Chemical Property of 1-Butanol, 4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-

Chemical Property:

• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 8
• Exact Mass: 328.185856666
• Heavy Atom Count: 23
• Complexity: 307

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CC(C)(C)[Si](C1=CC=CC=C1)(C2=CC=CC=C2)OCCCCO

Technology Process of 1-Butanol, 4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-

There total 12 articles about 1-Butanol, 4-[[(1,1-dimethylethyl)diphenylsilyl]oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

Butane-1,4-diol (110-63-4) + tert-butylchlorodiphenylsilane (58479-61-1) → 4-(tret-butyldiphenylsilyloxy)butan-1-ol (130372-07-5)

Guidance literature:

With dmap; triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 0 - 25 ℃;

DOI:10.1016/0040-4039(96)01165-3

Reference yield: 98.0%

C26H42O2Si2 → 4-(tret-butyldiphenylsilyloxy)butan-1-ol (130372-07-5)

Guidance literature:

sulfated SnO₂; In methanol; at 20 ℃; for 0.25h;

DOI:10.1080/00397910701767056

Reference yield: 91.0%

tert-butyl-diphenyl-[4-(tetrahydro-pyran-2-yloxy)-butoxy]-silane → 4-(tret-butyldiphenylsilyloxy)butan-1-ol (130372-07-5)

Guidance literature:

With tris-(4-bromophenyl)aminium hexachloroantimonate; In methanol; at 20 ℃; for 2.5h;

DOI:10.1016/j.tetlet.2008.03.149

upstream raw materials:

4-((tert-butyldiphenylsilyl)oxy)butanoic acid

Butane-1,4-diol

tert-butylchlorodiphenylsilane

1H-imidazole

Downstream raw materials:

4-(tert-butyldiphenylsiloxy)butyl methyl adipate

4-((tert-butyldiphenylsilyl)oxy)butanal

4-((tert-butyldiphenylsilyl)oxy)butanoic acid

2-[(tert-butyldiphenylsilyl)oxy]ethanol