(-)-(1S)-<(1α,2α,5α)-4,6,6-trimethylbicyclo<3.1.1>hept-3-en-2-yl> 2,6-dichlorobenzoate

Base Information

Chemical Name:(-)-(1S)-<(1α,2α,5α)-4,6,6-trimethylbicyclo<3.1.1>hept-3-en-2-yl> 2,6-dichlorobenzoate
CAS No.:144732-81-0
Molecular Formula:C₁₇H₁₈Cl₂O₂
Molecular Weight:325.235
Hs Code.:

Synonyms:(-)-(1S)-<(1α,2α,5α)-4,6,6-trimethylbicyclo<3.1.1>hept-3-en-2-yl> 2,6-dichlorobenzoate

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Chemical Property of (-)-(1S)-<(1α,2α,5α)-4,6,6-trimethylbicyclo<3.1.1>hept-3-en-2-yl> 2,6-dichlorobenzoate

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Technology Process of (-)-(1S)-<(1α,2α,5α)-4,6,6-trimethylbicyclo<3.1.1>hept-3-en-2-yl> 2,6-dichlorobenzoate

There total 1 articles about (-)-(1S)-<(1α,2α,5α)-4,6,6-trimethylbicyclo<3.1.1>hept-3-en-2-yl> 2,6-dichlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 473-67-6,1820-09-3,1845-30-3,5416-53-5,13040-03-4,18881-04-4,19890-02-9,22339-08-8,80795-83-1
trans-verbenol

: 4659-45-4
2,6-Dichlorobenzoyl chloride

: 144732-81-0
(-)-(1S)-<(1α,2α,5α)-4,6,6-trimethylbicyclo<3.1.1>hept-3-en-2-yl> 2,6-dichlorobenzoate

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1) THF, n-hexane, 0 deg C, 15 min, 2a) 0 deg C, 15 min, 2b) r.t., 30 min, 2c) 50 deg C, 4 h;
DOI:10.1016/S0040-4020(01)88263-6