octyl p-tolyl ketone

Base Information

Chemical Name:octyl p-tolyl ketone
CAS No.:168432-71-1
Molecular Formula:C₁₆H₂₄O
Molecular Weight:232.366
Hs Code.:

Synonyms:octyl p-tolyl ketone

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Chemical Property of octyl p-tolyl ketone

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Technology Process of octyl p-tolyl ketone

There total 12 articles about octyl p-tolyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 111-83-1
1-bromo-octane

: 104-87-0
4-methyl-benzaldehyde

: 168432-71-1
octyl p-tolyl ketone

Guidance literature:: 1-bromo-octane; With magnesium; In tetrahydrofuran; at 20 ℃; for 1h;

4-methyl-benzaldehyde; In tetrahydrofuran; at 0 - 20 ℃; for 2h;

With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate; In tetrahydrofuran; tert-butyl alcohol; for 20h; Reflux; Darkness;
DOI:10.1016/j.tet.2012.05.059

Reference yield: 62.0%

: 111-66-0,25068-25-1
oct-1-ene

: 104-87-0
4-methyl-benzaldehyde

: 168432-71-1
octyl p-tolyl ketone

Guidance literature:: With tert.-butylhydroperoxide; potassium tert-butylate; In decane; acetonitrile; at 100 ℃; for 12h; Schlenk technique;
DOI:10.1002/adsc.201400629

Reference yield:

: 629-27-6
1-Iodooctane

: 874-58-8
4-methylbenzoyl bromide

: 540-08-9
heptadecan-9-one

: 168432-71-1
octyl p-tolyl ketone

Guidance literature:: 4-methylbenzoyl bromide; With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran-d8; for 0.0833333h; Inert atmosphere; Glovebox; Sealed tube;

1-Iodooctane; With zinc; In tetrahydrofuran-d8; N,N-dimethyl acetamide; at 20 ℃; for 0.0833333h; Reagent/catalyst; Sealed tube;
DOI:10.1021/om5004682