(1S,2S)-tert-butyl 1-benzyl-2-(2,4,6-trimethylbenzylamino) cyclopentanecarboxylate

Base Information

Chemical Name:(1S,2S)-tert-butyl 1-benzyl-2-(2,4,6-trimethylbenzylamino) cyclopentanecarboxylate
CAS No.:1107613-46-6
Molecular Formula:C₂₇H₃₇NO₂
Molecular Weight:407.596
Hs Code.:

Synonyms:(1S,2S)-tert-butyl 1-benzyl-2-(2,4,6-trimethylbenzylamino) cyclopentanecarboxylate

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Chemical Property of (1S,2S)-tert-butyl 1-benzyl-2-(2,4,6-trimethylbenzylamino) cyclopentanecarboxylate

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Technology Process of (1S,2S)-tert-butyl 1-benzyl-2-(2,4,6-trimethylbenzylamino) cyclopentanecarboxylate

There total 1 articles about (1S,2S)-tert-butyl 1-benzyl-2-(2,4,6-trimethylbenzylamino) cyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: lithium N-mesitylmethyl-N-TMS-amide

: 27784-73-2
tert-butyl cyclopentene-1-carboxylate

: 100-39-0
benzyl bromide

: 1107613-46-6
(1S,2S)-tert-butyl 1-benzyl-2-(2,4,6-trimethylbenzylamino) cyclopentanecarboxylate

Guidance literature:: lithium N-mesitylmethyl-N-TMS-amide; With (1R,2R)-1,2-diphenyl-1,2-dimethoxyethane; In hexane; toluene; at -78 ℃; for 0.5h; Inert atmosphere;

tert-butyl cyclopentene-1-carboxylate; In hexane; toluene; at -78 - -60 ℃; for 3.08333h; Inert atmosphere;

benzyl bromide; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; toluene; at -40 ℃; for 1h; optical yield given as %ee; Inert atmosphere;
DOI:10.1021/ol802759j

Reference yield: 98.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 1107613-46-6
(1S,2S)-tert-butyl 1-benzyl-2-(2,4,6-trimethylbenzylamino) cyclopentanecarboxylate

: 1107613-58-0
(1S,2S)-tert-butyl 1-benzyl-2-(methyl(2,4,6-trimethylbenzyl)amino) cyclopentanecarboxylate

Guidance literature:: With water; sodium cyanoborohydride; In acetonitrile; at 20 ℃; for 0.25h; optical yield given as %ee;
DOI:10.1021/ol802759j