3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide

Base Information

Chemical Name:3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide
CAS No.:214286-81-4
Molecular Formula:C₂₁H₂₂FNO₂
Molecular Weight:339.41
Hs Code.:

Synonyms:3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide

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Chemical Property of 3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide

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Technology Process of 3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide

There total 3 articles about 3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116-11-0
2-Methoxypropene

: 3-(4-Fluoro-phenyl)-N-((1S,2R)-2-hydroxy-indan-1-yl)-propionamide

: 214286-81-4
3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide

Guidance literature:: With methanesulfonic acid; In dichloromethane; at 23 ℃; for 0.25h; Yield given;
DOI:10.1021/jm980537b

Reference yield:

: 459-31-4
3-(4-fluorophenyl)propanoic acid

: 214286-81-4
3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl chloride / dimethylformamide; benzene / 1.5 h / 23 °C

2: Et₃N / tetrahydrofuran / 0.33 h / 0 °C

3: methanesulfonic acid / CH₂Cl₂ / 0.25 h / 23 °C

With oxalyl dichloride; methanesulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm980537b

Reference yield:

: 772-70-3
3-(4-fluorophenyl)propanoyl chloride

: 214286-81-4
3-(4'-fluorophenyl)propionic acid cis-(1''S,2''R)-1''-amino-2''-indanolacetonide amide

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / tetrahydrofuran / 0.33 h / 0 °C

2: methanesulfonic acid / CH₂Cl₂ / 0.25 h / 23 °C

With methanesulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm980537b