methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate

Base Information

Chemical Name:methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate
CAS No.:1319721-57-7
Molecular Formula:C₂₇H₂₄O₇S
Molecular Weight:492.549
Hs Code.:

Synonyms:methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate

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Chemical Property of methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate

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Technology Process of methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate

There total 5 articles about methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1319721-55-5
phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

: 1319721-57-7
methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 5 h / 90 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

3: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 1 h

4: methanol; diethyl ether; dichloromethane / 0.33 h / 20 °C

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene;
DOI:10.1016/j.carres.2011.03.042

Reference yield:

: 1319721-75-9
C₂₆H₂₄O₆S

: 1319721-57-7
methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 1 h

2: methanol; diethyl ether; dichloromethane / 0.33 h / 20 °C

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1016/j.carres.2011.03.042

Reference yield:

: 1319721-74-8
C₄₆H₄₄N₂O₇S₂Si

: 1319721-57-7
methyl (phenyl 2,3-di-O-benzoyl-4-deoxy-1-thio-β-D-glucopyranoside)uronate

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / dichloromethane; water / 1 h

3: methanol; diethyl ether; dichloromethane / 0.33 h / 20 °C

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;
DOI:10.1016/j.carres.2011.03.042