phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

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Chemical Name:phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside
CAS No.:1319721-55-5
Molecular Formula:C₄₂H₄₂O₇SSi
Molecular Weight:718.943
Hs Code.:

Synonyms:phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 138857-50-8
phenyl 2,3-bis-O-benzoyl-1-thio-β-D-glucopyranoside

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1319721-55-5
phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 20h;
DOI:10.1016/j.carres.2011.03.042

Reference yield: 89.0%

: 1319721-55-5
phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

: 6160-65-2
1,1'-Thiocarbonyldiimidazole

: 1319721-74-8
C₄₆H₄₄N₂O₇S₂Si

Guidance literature:: In toluene; at 90 ℃; for 5h;
DOI:10.1016/j.carres.2011.03.042

Reference yield: 75.0%

: 1319721-55-5
phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside

: 6386-24-9
2,3,4,6-tetra-O-benzyl-D-galactopyranose

: 1338672-81-3
phenyl 2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl-(1->4)-2,3-di-O-benzoyl-6-O-tert-butyldiphenylsilyl-1-thio-β-D-glucopyranoside

Guidance literature:: 2,3,4,6-tetra-O-benzyl-D-galactopyranose; With bis(triphenyl)oxodiphosphonium trifluoromethanesulfonate salt; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.5h; Inert atmosphere;

phenyl 2,3-di-O-benzoyl-6-O-(tert-butyldiphenylsilyl)-1-thio-β-D-glucopyranoside; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 0.25h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/jo2015856