phenyliminobis(diisopropylamino)phosphine azide

Base Information

Chemical Name:phenyliminobis(diisopropylamino)phosphine azide
CAS No.:96455-33-3
Molecular Formula:C₁₈H₃₃N₆P
Molecular Weight:364.474
Hs Code.:

Synonyms:phenyliminobis(diisopropylamino)phosphine azide

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Chemical Property of phenyliminobis(diisopropylamino)phosphine azide

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Technology Process of phenyliminobis(diisopropylamino)phosphine azide

There total 2 articles about phenyliminobis(diisopropylamino)phosphine azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 56183-64-3
Azidophosphan

: 622-37-7
Phenyl azide

: 96455-33-3
phenyliminobis(diisopropylamino)phosphine azide

Guidance literature:: In benzene; at 80 ℃; for 2h;
DOI:10.1021/ja00299a033

Reference yield:

: 56183-63-2
bis(diisopropylamino)chlorophosphine

: 96455-33-3
phenyliminobis(diisopropylamino)phosphine azide

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / Me₃SiN₃ / benzene / 48 h / Ambient temperature

2: 90 percent / benzene / 2 h / 80 °C

With trimethylsilylazide; In benzene;
DOI:10.1021/ja00299a033